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12 Nov 2019
Can anyone identify this compound based off mass spec, C13 and H NMR?
Melting point = 121-123 degrees celsius
4.3 42 4.1 4,039 3ã37 363.524 1.9 1.8 1.7 16 IS 1.4 13 12 1.1 1.009 on or 3as 34 19 18 17 18 15 14 13 1.2 1.1 10 09 08 7 o Set 9, 63001-Mass Spectral Data Mass Intensity 27.e 38.e 39.e 50.e 51.0 1.2 2.3 6.3 4.4 100 53. 1.1 80 1.6 2.5 57.0 57.5 58.0 61.8 62.8 1.8 1.9 5.7 60 63. 11.e 64.8 2. 65.0 4.4 72.0 3.2 3.5 75.8 2.9 76. 1.4 40 74.e 20 1.1 2.1 87. 3.5 88.8 2.8 89.8 10.8 1.5 113. 2.6 114.8 3.9 115.0 70.7 116.8 24.1 1.9 77.0 86.8 100 125 150 25 50 75 98.e m/z 1.2 126.0 143. 1.3 144.8 180.8 145.0 18.9
Can anyone identify this compound based off mass spec, C13 and H NMR?
Melting point = 121-123 degrees celsius
4.3 42 4.1 4,039 3ã37 363.524 1.9 1.8 1.7 16 IS 1.4 13 12 1.1 1.009 on or 3as 34 19 18 17 18 15 14 13 1.2 1.1 10 09 08 7 o Set 9, 63001-Mass Spectral Data Mass Intensity 27.e 38.e 39.e 50.e 51.0 1.2 2.3 6.3 4.4 100 53. 1.1 80 1.6 2.5 57.0 57.5 58.0 61.8 62.8 1.8 1.9 5.7 60 63. 11.e 64.8 2. 65.0 4.4 72.0 3.2 3.5 75.8 2.9 76. 1.4 40 74.e 20 1.1 2.1 87. 3.5 88.8 2.8 89.8 10.8 1.5 113. 2.6 114.8 3.9 115.0 70.7 116.8 24.1 1.9 77.0 86.8 100 125 150 25 50 75 98.e m/z 1.2 126.0 143. 1.3 144.8 180.8 145.0 18.9