Question

From that procedure and data, what is the product loss and where does it occur?

OChem Experiment 6 - Word A Alexa May Miller -a File Home Insert Draw Design Layout References Mailings Review View Tell me what you want to do Share- Cut Copy Format Painter . A A Aa·~ ·-·-·-·느 느 의 T AaBbCcDa AaBbCcDd AaBbCC AaBbCcD AaB AaBbCcD Times New Roman 11 ac Replace :-. S. I. INormal |No Spec Heading 1 Heading 2 Title Subtitle Paste Select Clipboard Font Paragraph Styles Editing 2) m of dichlorometane into a Place 0.5 grams of benzoie acid pbenanthrene mixture and 10 beaker. Put the mixture from the beaker into a separatory lunnel when the mixture is completely dissolved 3) 4) Add 5m of MNaOH aqueous solution into the funnel then put in the stopper and mix the solutions together. 5) Allow the layers to separate. Then, drain the boto layer in the fnel iuto a tlask and the top layer into a separate flask. 6) Repeat steps 3-6. 7) Combine the two aqucous layers into one flask and then make the mixture acidie using pH paper and adding 1 MHC 8) Using an ice bath cool the acidic solution. 9) Then get the white precipitate by using vacuum filtration. 1 Put the precipitate on filter paper and wash with cold water, then allow the benzoic acid to dry 1화 Once dry, weigh with a scale and determine the melting point with a melting point apparatus. 12} Use CDC13 as a solvent and run the sample to get its NMR spectrum. 131 Over anhydrous sodium sullate, dry the compound. 14 Pour the solution fron one contaier to the other to remove tbe drying agent 15 Remove the dichloromethane from this solution by placing it in a round-bottom flask and connecting it to a rotary evaporator 16 Using a scale and melting point apparatus, find the melting point and the weigkt of the 17} Find the NMR spectrum of the phenanthrene, using CDC13 as a solvent. Page 3 of 5 681 words E 10:17 AM 3/7/2018 1